This work reports on synthesis of high yield (92%) of isosadeuterio-benzopinacol (benzopinacol-d20) via photo-reductive dimerization of benzophenone-d10. The latter compound was obtained using an improved method to achieve a material with high isotopic purity (> 99%). This material can be served for calibration of Mass spectrometric assays. In this study, it was also observed that benzophenone-d10 reacts faster than its natural abundance counterpart. However, elucidating the origin of this phenomenon will require additional work.
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Author Name: Steeve M. Adjibodéa; Urbain C. Kasséhin; Fernand A. Gbaguidi; Jacques H. Poupaert
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Keywords: Benzopinacol-d20 Benzophenone-d10 Dimerization Photo-reductive
ISSN: 2651-4702
EISSN:
EOI/DOI: 10.26655/JMCHEMSCI.2020.1.4
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